LCMS data
| Crude drug latin name | CINNAMOMI CORTEX | |
| Sample | NIB-0014 | |
| CHROM_NAME | APCI-Orbitrap(-) | |
| CHROM_TYPE | LC | |
| LC MACHINE TYPE | Shimadzu UFLC | |
| MS MACHINE TYPE | ThermoFisher Scientific LTQ Orbitrap XL | |
| Column | FILTER | ODS |
| LENGTH | 150mm | |
| DIAMETER | 4.6mm | |
| PARTICLES_SIZE | 2.0μm | |
| MANUFACTURER | GL science | |
| PRODUCT_NAME | Inertsil ODS-4 | |
| LC Measurement condition | MOBILE_PHASE | A = 0.1% (v/v) acetic acid in ultrapure water; B = 0.1% (v/v) acetic acid in acetonitrile |
| LC_G_PROGRAM | B = 5 - 70 % (30 min) – 100 % (35 min) – 100 % (38 min) | |
| COLUMN_TEMP | 40℃ | |
| FLOW_RATE | 0.8 mL/min | |
| MS Measurement condition | Ionization mode | negative |
| Desolvationtemperature | 300 ℃ | |
| Needle voltage | ||
| Velocity of Spectrum | ||
| Range of m/z | 100-2000 | |
| Collision gas | He | |
| TIC_JCAMP_FILE |  NIB-0014(-).jdx | |
| 3D(PDA) data | ||
| UV data | ||
| MEMO | sample: KEIHI(Cinnamon Bark) water ext. 1 mg/mL (methanol) Injection Volume: 10μL(pos.), 30μL(neg.) ケイヒ 水抽出エキス 1 mg/mL (メタノール溶液) 注入量： 10μL(positiveモード), 30μL(negativeモード) | |
| MS data list | ||